N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

Base Information

Chemical Name:N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide
CAS No.:1314069-43-6
Molecular Formula:C₁₈H₂₂BFN₂O₄S
Molecular Weight:392.259
Hs Code.:

Synonyms:N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

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Chemical Property of N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

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Technology Process of N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

There total 3 articles about N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 928140-28-7
pyridin-3-ylmethanesulfonyl chloride trifluoromethanesulfonate

: 819058-34-9
2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

: 1314069-43-6
N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

Guidance literature:: pyridin-3-ylmethanesulfonyl chloride trifluoromethanesulfonate; 2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline; With pyridine; for 18h; Inert atmosphere;

With sulfuryl dichloride; for 24h;

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 1314069-43-6
N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 4.5 h / 85 °C / Inert atmosphere

2.1: pyridine / 18 h / Inert atmosphere

2.2: 24 h

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide;

Reference yield:

: 29632-74-4
2-fluro-4-iodoaniline

: 1314069-43-6
N-[2-fluoro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(pyridin-3-yl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 4.5 h / 85 °C / Inert atmosphere

2.1: pyridine / 18 h / Inert atmosphere

2.2: 24 h

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide;