1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

Base Information

Chemical Name:1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on
CAS No.:357396-87-3
Molecular Formula:C₃₅H₅₂I₂O₅
Molecular Weight:806.604
Hs Code.:

Synonyms:1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

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Chemical Property of 1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

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Technology Process of 1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

There total 6 articles about 1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 357396-85-1
1-(3,4-dihexyloxyphenyl)-5-bromo-pentan-1-one

: 357396-86-2
4-(hexyloxy)-2,5-diiodophenol

: 357396-87-3
1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

Guidance literature:: With potassium carbonate; In various solvent(s); for 16h; Heating;
DOI:10.1021/ja015614y

Reference yield:

: 111-25-1
1-bromo-hexane

: 357396-87-3
1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / KOH

2: 88 percent / AlCl₃ / CS₂ / 0 - 40 °C

3: 93 percent / potassium carbonate / various solvent(s) / 16 h / Heating

With potassium hydroxide; aluminium trichloride; potassium carbonate; In carbon disulfide; 2: Friedel-Crafts acylation;
DOI:10.1021/ja015614y

Reference yield:

: 94259-20-8
1,2-dihexyloxybenzene

: 357396-87-3
1-(3,4-bis-hexyloxy-phenyl)-5-(4-hexyloxy-2,5-diiodo-phenoxy)-pentane-1-on

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / AlCl₃ / CS₂ / 0 - 40 °C

2: 93 percent / potassium carbonate / various solvent(s) / 16 h / Heating

With aluminium trichloride; potassium carbonate; In carbon disulfide; 1: Friedel-Crafts acylation;
DOI:10.1021/ja015614y