1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

Base Information

Chemical Name:1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline
CAS No.:374633-75-7
Molecular Formula:C₂₉H₂₄N₄O₂
Molecular Weight:460.535
Hs Code.:

Synonyms:1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

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Chemical Property of 1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

Chemical Property:

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Technology Process of 1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

There total 6 articles about 1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3,4-Methylenedioxyphenyl)-2-[5-(4-methoxyphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-δ-carboline

: 120908-70-5,125707-25-7
1-(3,4-methylenedioxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 27956-37-2
2-chloro-5-(4-methyl phenyl)pyrimidine

: 374633-75-7
1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene;

Reference yield:

: 120908-70-5,125707-25-7
1-(3,4-methylenedioxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 27956-37-2
2-chloro-5-(4-methyl phenyl)pyrimidine

: 374633-75-7
1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 120 ℃;
DOI:10.1016/S0960-894X(02)01036-3

Reference yield:

: 61-54-1
tryptamine

: 374633-75-7
1-(3,4-methylenedioxyphenyl)-2-[5-(4-methylphenyl)-pyrimidin-2-yl]-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂

2: DIEA / dimethylformamide / 120 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)01036-3