2-chloro-N-(2-chloro-4-methylphenyl)acetamide

Base Information

• Chemical Name: 2-chloro-N-(2-chloro-4-methylphenyl)acetamide
• CAS No.: 379255-38-6
• Molecular Formula: C₉H₉Cl₂NO
• Molecular Weight: 218.083
• DSSTox Substance ID: DTXSID501254952
• Mol file: 379255-38-6.mol

Synonyms:2-chloro-N-(2-chloro-4-methylphenyl)acetamide;379255-38-6;SCHEMBL7264600;DTXSID501254952;MFCD03147357;STK482951;AKOS000266297;BS-10272;EN300-01643;Z56896249

Chemical Property of 2-chloro-N-(2-chloro-4-methylphenyl)acetamide

Chemical Property:

• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 217.0061193
• Heavy Atom Count: 13
• Complexity: 187

Purity/Quality:

98%min ^*data from raw suppliers

2-Chloro-N-(2-chloro-4-methylphenyl)acetamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)NC(=O)CCl)Cl

Technology Process of 2-chloro-N-(2-chloro-4-methylphenyl)acetamide

There total 2 articles about 2-chloro-N-(2-chloro-4-methylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

chloroacetyl chloride (79-04-9) + 2-chloro-4-methyl-benzenamine (615-65-6) → 2-chloro-N-(2-chloro-4-methylphenyl)acetamide (379255-38-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2013.12.045

Reference yield:

→ 2-chloro-N-(2-chloro-4-methylphenyl)acetamide (379255-38-6)

Guidance literature:

With sodium acetate; acetic acid; In water; at 20 ℃;

Reference yield: 80.0%

2-chloro-N-(2-chloro-4-methylphenyl)acetamide (379255-38-6) + 6-chloro-1-(3,5-dimethylbenzyl)-1,3-dihydro-2H-benzimidazole-2-thione (1061732-18-0) → C25H23Cl2N3OS (1562665-37-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2013.12.045

upstream raw materials:

chloroacetyl chloride

2-chloro-4-methyl-benzenamine

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