bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide]

Base Information

• Chemical Name: bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide]
• CAS No.: 133644-59-4
• Molecular Formula: C₂₀H₅₂CaN₂O₂Si₄
• Molecular Weight: 505.065
• Mol file: 133644-59-4.mol

Synonyms:bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide]

Chemical Property of bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide]

There total 1 articles about bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

C45H67CaN5OSi2*C7H8 → bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide] (133644-59-4) + 2C35H41N4(1-)*Ca(2+)

Guidance literature:

In hexane; at 20 ℃; for 168h;

DOI:10.1021/acs.inorgchem.8b00088

Reference yield: 95.0%

bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide] (133644-59-4) + 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole (1366268-40-7) → C34H42CaN4O2 (1366268-38-3)

Guidance literature:

In toluene; at 90 ℃; for 12h; Inert atmosphere;

DOI:10.1021/om201210y

Reference yield: 93.0%

bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide] (133644-59-4) + 1,3-bis(2,4,6-trimethylphenyl)triazene → C44H60CaN6O2

Guidance literature:

In toluene; for 3h;

DOI:10.1039/c5dt00595g

Downstream raw materials:

C₃₄H₅₆CaN₆O₂

[(CH2(C(CH2)NC6H3(CH(CH3)2)2)2)Al(CH3)(μ-O)Ca(tetrahydrofuran)]2

C₄₂H₅₈CaN₄O₂

C₃₁H₅₅CaN₃O₂Si₂