2?{1?[(4?methylphenyl)imino]ethyl}pyrrole

Base Information

• Chemical Name: 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole
• CAS No.: 1366268-40-7
• Molecular Formula: C₁₃H₁₄N₂
• Molecular Weight: 198.268
• Mol file: 1366268-40-7.mol

Synonyms:2?{1?[(4?methylphenyl)imino]ethyl}pyrrole

Chemical Property of 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole

There total 1 articles about 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.9%

2-Acetylpyrrole (1072-83-9) + p-toluidine (106-49-0,12221-03-3) → 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole (1366268-40-7)

Guidance literature:

In acetic acid; for 0.0833333h; Inert atmosphere; Schlenk technique; UV-irradiation;

DOI:10.1134/S1070328420050073

Reference yield: 95.0%

bis(tetrahydrofuran)calcium-bis[bis(trimethylsilyl)amide] (133644-59-4) + 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole (1366268-40-7) → C34H42CaN4O2 (1366268-38-3)

Guidance literature:

In toluene; at 90 ℃; for 12h; Inert atmosphere;

DOI:10.1021/om201210y

Reference yield: 88.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 2?{1?[(4?methylphenyl)imino]ethyl}pyrrole (1366268-40-7) → C34H42MgN4O2 (1366268-39-4)

Guidance literature:

2-{1-[(4-methylphenyl)imino]-ethyl}pyrrole; With dibenzylmagnesium; In toluene; at 90 ℃; for 12h; Inert atmosphere;

tetrahydrofuran; In pentane; at -35 ℃;

DOI:10.1021/om201210y

upstream raw materials:

2-Acetylpyrrole

p-toluidine

Downstream raw materials:

C₃₄H₄₂MgN₄O₂

C₃₄H₄₂CaN₄O₂