trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium

Base Information

• Chemical Name: trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium
• CAS No.: 866343-83-1
• Molecular Formula: C₆₀H₅₃ClN₂P₂Pd
• Molecular Weight: 1005.91

Synonyms:trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium

Chemical Property of trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium

There total 2 articles about trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium (713524-71-1) + aniline (62-53-3) → trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium (866343-83-1)

Guidance literature:

With oxygen; In acetonitrile; byproducts: H2O; refluxing a soln. of palladium complex and amine in acetonitrile under O2;

DOI:10.1021/ja052780n

Reference yield:

[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chloropalladium (866343-80-8) + triphenylphosphine (603-35-0) → trans-[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chlorobis(triphenylphosphine)palladium (866343-83-1)

Guidance literature:

In chloroform-d1; addn. of phosphine to a soln. of palladium complex in CDCl3; detected by NMR;

DOI:10.1021/ja052780n

upstream raw materials:

[4-tert-butyl-2,6-bis(N-phenylimino)phenyl]chloropalladium

triphenylphosphine

trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

aniline

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