trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

Base Information

Chemical Name:trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium
CAS No.:713524-71-1
Molecular Formula:C₄₈H₄₃ClO₂P₂Pd
Molecular Weight:855.689
Hs Code.:

Synonyms:trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

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Chemical Property of trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

Chemical Property:

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Technology Process of trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

There total 1 articles about trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52522-40-4
tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex

: 603-35-0
triphenylphosphine

: lithium chloride

: 713524-75-5
4-(tert-butyl)-2,6-diformylphenyl trifluoromethanesulfonate

: 713524-71-1
trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

Guidance literature:: In not given;
DOI:10.1021/ja052780n

Reference yield: 98.0%

: 713524-71-1
trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

: 25746-83-2,64030-43-9,104261-87-2
(2S)-N-phenylpyrrolidine-2-carboxamide

: [4-tert-butyl-2,6-bis((3R,7aS)-2-phenylhexahydro-1H-pyrrolo[1,2-c]imidazol-1-on-3-yl)phenyl]chloropalladium

Guidance literature:: With oxygen; In acetonitrile; byproducts: H2O, (C6H5)3PO; refluxing a soln. of palladium complex and amine in acetonitrile under O2, cooling to room temp.; evapn., column chromy. (silica gel);
DOI:10.1021/ja052780n

Reference yield: 92.0%

: 713524-71-1
trans-(4-tert-butyl-2,6-difolmylphenyl)chlorobis(triphenylphosphine)-palladium

: 108-91-8,157973-60-9
cyclohexylamine

: 866343-74-0
[4-tert-butyl-2,6-bis(N-cyclohexylimino)phenyl]chloropalladium

Guidance literature:: With oxygen; In acetonitrile; byproducts: H2O, (C6H5)3PO; refluxing a soln. of palladium complex and amine in acetonitrile under O2, cooling to room temp.; evapn., column chromy. (silica gel);
DOI:10.1021/ja052780n