Technology Process of C71H44
There total 8 articles about C71H44 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Aliquat 336; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
water; toluene;
at 100 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / toluene; ethanol; water / 12 h / Reflux
2: N-Bromosuccinimide / dichloromethane / 5 h / 20 °C
3: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 100 °C
With
N-Bromosuccinimide; Aliquat 336; sodium carbonate; potassium carbonate;
bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0);
In
ethanol; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: magnesium / diethyl ether / 3 h / Reflux
1.2: 12 h / Reflux
2.1: hydrogenchloride / 4 h / Reflux
3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; diethylene glycol / 12 h / 80 °C
4.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C
4.2: -78 - 25 °C
5.1: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 6 h / 100 °C
With
hydrogenchloride; n-butyllithium; Aliquat 336; potassium carbonate; magnesium;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; hexane; water; toluene; diethylene glycol;