glutaric acid dimenthyl ester

Base Information

• Chemical Name: glutaric acid dimenthyl ester
• CAS No.: 77304-30-4
• Molecular Formula: C₂₅H₄₄O₄
• Molecular Weight: 408.622
• Mol file: 77304-30-4.mol

Synonyms:glutaric acid dimenthyl ester

Chemical Property of glutaric acid dimenthyl ester

Chemical Property:

Purity/Quality:

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Technology Process of glutaric acid dimenthyl ester

There total 5 articles about glutaric acid dimenthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

glutaric anhydride, (108-55-4) + menthol (89-78-1) → glutaric acid dimenthyl ester (77304-30-4)

Guidance literature:

With dmap; In toluene; at 125 ℃;

Reference yield:

glutaric anhydride, (108-55-4) + (-)-menthol (2216-51-5) → glutaric acid di-(-)menthyl ester (77304-30-4) + mono-L-menthyl glutarate (220621-22-7)

Guidance literature:

sodium carbonate; at 70 - 110 ℃; for 2.8 - 30h; Product distribution / selectivity;

Reference yield:

glutaric anhydride, (108-55-4) + (-)-menthol (2216-51-5) → 1,5-pentanedioic acid (110-94-1) + glutaric acid monomenthyl ester (406179-70-2) + glutaric acid dimenthyl ester (77304-30-4)

Guidance literature:

With sodium carbonate; at 90 ℃; for 5h;

upstream raw materials:

gloutaric dichloride

(-)-menthol

glutaric anhydride,

1,5-pentanedioic acid

Downstream raw materials:

glutaric acid monomenthyl ester