tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

Base Information

Chemical Name:tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate
CAS No.:1351691-91-2
Molecular Formula:C₃₁H₃₃N₅O₅
Molecular Weight:555.634
Hs Code.:

Synonyms:tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

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Chemical Property of tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

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Technology Process of tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

There total 1 articles about tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1328921-95-4
C₁₄H₁₆O₃

: 1351691-90-1
C₁₇H₁₉N₅O₃

: 1351691-91-2
tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

Guidance literature:: C₁₄H₁₆O₃; C₁₇H₁₉N₅O₃; With triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With di-isopropyl azodicarboxylate; In tetrahydrofuran; at 20 ℃; for 0.666667h;

Reference yield: 50.0%

: 1351691-91-2
tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate

: 142217-69-4,76704-05-7
entecavir

Guidance literature:: tert-butyl 6-(benzyloxy)-9-((4aR,6S,7aS)-5-methylene-2-phenylhexahydrocyclopenta[d][1,3]dioxin-6-yl)-9H-purin-2-ylcarbamate; With hydrogenchloride; water; In dichloromethane; at 20 ℃; for 18h;

With sodium hydroxide; at 20 ℃; for 0.75h; pH=7 - 8;