4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

Base Information

Chemical Name:4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene
CAS No.:1198166-34-5
Molecular Formula:C₂₁H₂₁F₆IO₃
Molecular Weight:562.291
Hs Code.:

Synonyms:4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

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Chemical Property of 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

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Technology Process of 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

There total 3 articles about 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1198166-33-4
4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-propylphenoxy)-2-methylaniline

4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene: 1198166-34-5
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 0 - 10 ℃;
DOI:10.1016/j.bmc.2016.05.048

Reference yield:

: 1198166-32-3
2-methyl-4-[2-n-propyl-4-(2,2,2-trifluoro-1-methoxymethoxy-1-trifluoromethylethyl)phenoxy]-1-nitrobenzene

4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene: 1198166-34-5
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

2: potassium iodide; toluene-4-sulfonic acid; sodium nitrite / water; acetonitrile / 0 - 10 °C

With palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In methanol; water; acetonitrile;
DOI:10.1016/j.bmc.2016.05.048

Reference yield:

: 1031393-25-5
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenol

4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene: 1198166-34-5
4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-(4-iodo-3-methylphenoxy)-2-n-propylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

2: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

3: potassium iodide; toluene-4-sulfonic acid; sodium nitrite / water; acetonitrile / 0 - 10 °C

With palladium on activated charcoal; hydrogen; potassium carbonate; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2016.05.048