ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

Base Information

Chemical Name:ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate
CAS No.:114371-49-2
Molecular Formula:C₁₈H₃₁NO₄
Molecular Weight:325.448
Hs Code.:

ethyl <S-(E)>-5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

Synonyms:ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

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Chemical Property of ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

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Technology Process of ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

There total 3 articles about ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98105-42-1
(S)-2-(t-butoxycarbonylamino)-3-cyclohexyl-1-propanal

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 114371-49-2
ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

Guidance literature:: In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00105a022

Reference yield:

: 103322-56-1
tert-butyl [(1S)-2-cyclohexyl-1-(hydroxymethyl)ethyl]carbamate

: 114371-49-2
ethyl -5-cyclohexyl-4-<<(1,1-dimethylethoxy)carbonyl>amino>-2-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 25 °C

2: benzene / 0.5 h / 30 °C

With Dess-Martin periodane; In dichloromethane; benzene; 1: Oxidation / 2: olefination; Wittig reaction;
DOI:10.1021/jo991065r