tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Base Information

Chemical Name:tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate
CAS No.:1270084-25-7
Molecular Formula:C₃₁H₂₇N₃O₃
Molecular Weight:489.574
Hs Code.:

Synonyms:tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Suppliers and Price of tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

There total 4 articles about tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1270083-97-0
t-butyl 3-(3-iodophenyl)-1-(pyridin-2-yl)-1H-pyrazol-5-yl carbonate

: 5122-95-2
3-Biphenylboronic acid

: 1270084-25-7
tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; In 1,4-dioxane; at 100 ℃; for 1h;
DOI:10.1055/s-0030-1260018

Reference yield: 90.0%

: 1270084-25-7
tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Guidance literature:

Reference yield:

: 1270083-87-8
3-(3-iodophenyl)-1-(pyridin-2-yl)-1H-pyrazol-5-ol

: 1270084-25-7
tert-butyl 1-(2-pyridinyl)-3-[3-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane

2: potassium phosphate; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1 h / 100 °C

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; In 1,4-dioxane; dichloromethane; 2: Suzuki-Miyaura cross-coupling;
DOI:10.1055/s-0030-1260018