{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

Base Information

Chemical Name:{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4
CAS No.:131458-16-7
Molecular Formula:C₂₄H₂₀B*C₄₂H₄₅P₄Ru
Molecular Weight:1094.02
Hs Code.:

Synonyms:{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

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Chemical Property of {cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

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Technology Process of {cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

There total 1 articles about {cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: Ru⁽²⁺⁾*P(C₂H₄P(C₆H₅)2)3*C₂C₆H₅^(1-)*B(C₆H₅)4^(1-)*C₄H₈O

: 131458-16-7
{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

Guidance literature:: With hydrogen; In tetrahydrofuran; byproducts: styrene; soln. of complex, H2 (1 atm) heated t 60° for 30 min, colour change from red to yellow; addn. of EtOH, partial evapn. of solvent under N2, ppt.;

Reference yield: 90.0%

: 131458-16-7
{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

: 74-85-1
ethene

: 187280-21-3
[(P(CH2CH2PPh2)3)Ru(H)(η(2)-C2H4)][BPh4]

Guidance literature:: In tetrahydrofuran; absence of air and moisture; bubbling C2H4 at room temp. for 30 min; EtOH addn., concn. (pptn.); elem. anal.;
DOI:10.1021/ic960736q

Reference yield: 65.0%

: 131458-16-7
{cis-hydrido(η2-dihydrogen)(PP3)Ru}BPh4

: 536-74-3
phenylacetylene

: Ru⁽²⁺⁾*P(C₂H₄P(C₆H₅)2)3*C₂C₆H₅^(1-)*B(C₆H₅)4^(1-)*C₄H₈O

Guidance literature:: In tetrahydrofuran; byproducts: styrene; mixt. of hydrido-dihydrogen complex and PhC2H (protecting atmosphere, molar ratio 1:3), stirred (0°, 30 min), soln. changed from pale yellow to deep red; EtOH added, soln. concd.; elem. anal.;