Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

Base Information

Chemical Name:Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala
CAS No.:478363-03-0
Molecular Formula:C₅₆H₉₂N₈O₁₅
Molecular Weight:1117.39
Hs Code.:

Synonyms:Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

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Chemical Property of Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

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Technology Process of Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

There total 3 articles about Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 478363-01-8
Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala-OBn

: 478363-03-0
Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

Guidance literature:: With hydrogen; palladium on activated charcoal; In dichloromethane; for 2h; under 760.051 Torr;
DOI:10.1021/np020117w

Reference yield:

: 187807-02-9
C₅₂H₈₀N₆O₁₂

: 478363-03-0
Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / CH₂Cl₂ / 2 h / 760.05 Torr

2: 79 percent / i-Pr₂NEt; O-benzotriazol-1-yl-N,N,N',N'-tetramethyluronium BF₄ / dimethylformamide / 20 h

3: 99 percent / H₂ / Pd/C / CH₂Cl₂ / 2 h / 760.05 Torr

With hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/np020117w

Reference yield:

: 478362-98-0
C₄₅H₇₄N₆O₁₂

: 478363-03-0
Boc-Map-Hmp-Gly-N-Me-L-Leu-Gly-N-Me-L-Val-O,N-diMe-L-Tyr-Ibu-N-Me-L-Ala

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / i-Pr₂NEt; O-benzotriazol-1-yl-N,N,N',N'-tetramethyluronium BF₄ / dimethylformamide / 20 h

2: 99 percent / H₂ / Pd/C / CH₂Cl₂ / 2 h / 760.05 Torr

With hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/np020117w