2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

Base Information

Chemical Name:2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide
CAS No.:128425-55-8
Molecular Formula:C₂₀H₂₃N₃O₄S₂
Molecular Weight:433.552
Hs Code.:

Synonyms:2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

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Technology Process of 2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

There total 1 articles about 2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 941-55-9
4-toluenesulfonyl azide

: 40713-75-5
2-methyl-4-(1-pyrrolidinyl)-2H-1,2-benzothiazine 1,1-dioxide

: 128425-56-9
2-methyl-3-(1-pyrrolidinyl)-4-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

: 128425-55-8
2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

Guidance literature:: In benzene; at 80 ℃; for 7h;
DOI:10.1002/jhet.5570270260

Reference yield: 80.0%

: 128425-55-8
2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

: 128425-57-0
2-methyl-3-tosylamino-2H-1,2-benzothiazin-4-(3H)-one 1,1-dioxide

Guidance literature:: With sulfuric acid; In ethanol; for 12h; Ambient temperature;
DOI:10.1002/jhet.5570270260

Reference yield:

: 128425-55-8
2-methyl-4-(1-pyrrolidinyl)-3-tosylamino-2H-1,2-benzothiazine 1,1-dioxide

: 128425-59-2
2-methyl-3-tosylamino-3,4-dihydro-2H-1,2-benzothiazine 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 15percent aq. H₂SO₄ / ethanol / 12 h / Ambient temperature

2: 86 percent / NaBH₄ / ethanol / 2 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; In ethanol;
DOI:10.1002/jhet.5570270260