2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

Base Information

Chemical Name:2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)
CAS No.:1254177-33-7
Molecular Formula:C₃₇H₉Br₈F₆MnN₄
Molecular Weight:1317.67
Hs Code.:

Synonyms:2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

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Chemical Property of 2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

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Technology Process of 2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

There total 3 articles about 2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1254177-29-1
5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

: 1254177-33-7
2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

Guidance literature:: With bromine; In methanol; at 20 ℃;
DOI:10.1021/ja1050296

Reference yield: 60.0%

: 1254177-29-1
5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

: 7726-95-6
bromine

: 1254177-33-7
2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

Guidance literature:: In methanol; addn. of methanolic soln. of bromine to methanolic soln. of manganese compd., stirring at room temp. overnight; evapn. at room temp., chromy. (silica gel, hexane/ethyl acetate (10:1)),MS and UV;
DOI:10.1021/ja1050296

Reference yield:

: 1254177-43-9
2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato(oxo)manganese(V)

: 1254177-33-7
2,3,7,8,12,13,17,18-octabromo-5,10,15-tris(2,6-difluorophenyl)corrolato-manganese(III)

Guidance literature:: With BrC₆H₄SCH₃; In dichloromethane; byproducts: BrC6H4S(O)CH3; mixing CH2Cl2 acetate solns. of manganese compd. and bromothioanisole at20°C; UV monitoring; Kinetics;
DOI:10.1021/ja1050296