Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Base Information

Chemical Name:Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside
CAS No.:142890-58-2
Molecular Formula:C₂₄H₂₈O₅S₂
Molecular Weight:460.615
Hs Code.:

Synonyms:Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Suppliers and Price of Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

There total 4 articles about Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 618-32-6
Benzoyl bromide

: 142890-45-7
Methyl 5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

: 142890-58-2
Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; paraffin; for 4h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90576-7

Reference yield:

: 14645-49-9
methyl 2,3-anhydro-5-O-benzyl-α-D-lyxofuranoside

: 142890-58-2
Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) THF, hexane, -20 deg C, 2.5 h, 2.) THF, r.t., 3 h

2: 66 percent / 50percent NaH / dimethylformamide; paraffin / 4 h / Ambient temperature

With n-butyllithium; sodium hydride; In N,N-dimethyl-formamide; paraffin;
DOI:10.1016/S0008-6215(00)90576-7

Reference yield:

: 100-39-0
benzyl bromide

: 142890-58-2
Methyl 2-O-benzoyl-5-O-benzyl-3-deoxy-3-(1,3-dithian-2-yl)-α-D-arabino-pentofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 50percent NaH / dimethylformamide; paraffin / 4 h / Ambient temperature

2: 1.) BuLi / 1.) THF, hexane, -20 deg C, 2.5 h, 2.) THF, r.t., 3 h

3: 66 percent / 50percent NaH / dimethylformamide; paraffin / 4 h / Ambient temperature

With n-butyllithium; sodium hydride; In N,N-dimethyl-formamide; paraffin;
DOI:10.1016/S0008-6215(00)90576-7