methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

Base Information

Chemical Name:methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate
CAS No.:912942-91-7
Molecular Formula:C₁₈H₂₄O₇
Molecular Weight:352.384
Hs Code.:

Synonyms:methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

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Technology Process of methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

There total 2 articles about methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 912942-93-9
methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-5-oxo-α-D-ribo-heptofuranuronate

: 912942-91-7
methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

Guidance literature:: With (S)-BinapRuBr₂; hydrogen; In methanol; at 45 ℃; for 24h; under 760 Torr;
DOI:10.1016/j.tetasy.2006.07.022

Reference yield:

: 120417-90-5
1,2-O-(methylethylidene)-3-O-(phenylmethyl)-α-D-ribofuranuroic acid

: 912942-91-7
methyl 3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-allo-heptofuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 16 h / 20 °C

1.2: 58 percent / tetrahydrofuran / 20 °C

2.1: 80 percent / [((S)-Binap)RuBr₂]; hydrogen / methanol / 24 h / 45 °C / 760 Torr

With (S)-BinapRuBr₂; hydrogen; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2006.07.022