(-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

Base Information

Chemical Name:(-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate
CAS No.:1001017-66-8
Molecular Formula:C₂H₂O₄*C₃₂H₃₆N₂O₂
Molecular Weight:570.686
Hs Code.:

(-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

Synonyms:(-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

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Chemical Property of (-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

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Technology Process of (-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

There total 1 articles about (-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1001017-61-3
(1S,2R)-N-benzyl-2-(bromomethyl)-1-phenylcyclopropanecarboxamide

: 144-62-7,97993-78-7
oxalic acid

: 16603-67-1
(2R,6R,11R)-6,11-dimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocin-8-ol

: 1001017-66-8
(-)-(1S,2R)-N-benzyl-2-{[(2R,6R,11R)-8-hydroxy-6,11-dimethyl-1,4,5,6-tetrahydro-2,6-methano-3-benzazocin-3(2H)-yl]methyl}-1-phenylcyclopropanecarboxamide oxalate

Guidance literature:: (1S,2R)-N-benzyl-2-(bromomethyl)-1-phenylcyclopropanecarboxamide; (2R,6R,11R)-6,11-dimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benzo[d]azocin-8-ol; With sodium hydrogencarbonate; potassium iodide; In butanone; at 60 ℃; for 18h;

oxalic acid; In tetrahydrofuran;
DOI:10.1691/ph.2007.11.7523