4,4-dimethyl-5-hexenethioic acid p-tolylamide

Base Information

Chemical Name:4,4-dimethyl-5-hexenethioic acid p-tolylamide
CAS No.:1307292-85-8
Molecular Formula:C₁₅H₂₁NS
Molecular Weight:247.404
Hs Code.:

Synonyms:4,4-dimethyl-5-hexenethioic acid p-tolylamide

Suppliers and Price of 4,4-dimethyl-5-hexenethioic acid p-tolylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4-dimethyl-5-hexenethioic acid p-tolylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4-dimethyl-5-hexenethioic acid p-tolylamide

There total 4 articles about 4,4-dimethyl-5-hexenethioic acid p-tolylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 70472-96-7
5-bromo-3,3-dimethyl-pent-1-ene

: 622-59-3
1-isothiocyanato-4-methylbenzene

: 1307292-85-8
4,4-dimethyl-5-hexenethioic acid p-tolylamide

Guidance literature:: 5-bromo-3,3-dimethyl-pent-1-ene; With magnesium; iodine; In tetrahydrofuran; for 1h; Reflux;

1-isothiocyanato-4-methylbenzene; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 53589-56-3
3,3-dimethyl-4-pentenol

: 1307292-85-8
4,4-dimethyl-5-hexenethioic acid p-tolylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.1: lithium bromide / tetrahydrofuran / 2 h / Reflux

3.1: magnesium / iodine / tetrahydrofuran / 1 h / Reflux

3.2: 1 h / 0 - 20 °C

With magnesium; triethylamine; lithium bromide; iodine; In tetrahydrofuran;

Reference yield:

: 131922-42-4
3,3-dimethylpent-4-en-1-yl methanesulfonate

: 1307292-85-8
4,4-dimethyl-5-hexenethioic acid p-tolylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium bromide / tetrahydrofuran / 2 h / Reflux

2.1: magnesium / iodine / tetrahydrofuran / 1 h / Reflux

2.2: 1 h / 0 - 20 °C

With magnesium; lithium bromide; iodine; In tetrahydrofuran;