9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine

Base Information

• Chemical Name: 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine
• CAS No.: 389089-98-9
• Molecular Formula: C₄₂H₄₁N₅O₉
• Molecular Weight: 759.816

Synonyms:9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine

Chemical Property of 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine

Chemical Property:

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Technology Process of 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine

There total 1 articles about 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrguanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) + N-(9-{5-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-3,4-dihydroxy-tetrahydro-pyran-2-yl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide → 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N2-isobutyrguanine (389089-98-9)

Guidance literature:

In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/S0968-0896(01)00220-6

Reference yield: 70.0%

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) + 9-[2'-O-benzoyl-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N2-isobutyrguanine (389089-98-9) → 9-[2'-O-benzoyl-3'-O-((2-cyanoethoxy)(diisopropylamino)phosphino)-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N2-isobutyrylguanine (253875-10-4)

Guidance literature:

With 1-methyl-1H-imidazole; 2,4,6-trimethyl-pyridine; In dichloromethane; at 20 ℃;

DOI:10.1016/S0968-0896(01)00220-6

upstream raw materials:

benzoyl chloride

Downstream raw materials:

9-[2'-O-benzoyl-3'-O-((2-cyanoethoxy)(diisopropylamino)phosphino)-4'-O-((4'',4'''-dimethoxytriphenyl)methyl)-α-lyxopyranosyl-(1')]-N²-isobutyrylguanine

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