C₄₁H₄₇Cl₆NO₁₆

Base Information

Chemical Name:C₄₁H₄₇Cl₆NO₁₆
CAS No.:178247-85-3
Molecular Formula:C₄₁H₄₇Cl₆NO₁₆
Molecular Weight:1022.54
Hs Code.:

C<sub>41</sub>H<sub>47</sub>Cl<sub>6</sub>NO<sub>16</sub>

Synonyms:C₄₁H₄₇Cl₆NO₁₆

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Chemical Property of C₄₁H₄₇Cl₆NO₁₆

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Technology Process of C₄₁H₄₇Cl₆NO₁₆

There total 9 articles about C₄₁H₄₇Cl₆NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 178247-84-2
C₄₉H₅₉Cl₆NO₁₈

: 178247-85-3
C₄₁H₄₇Cl₆NO₁₆

Guidance literature:: With formic acid; for 2h; Ambient temperature;
DOI:10.1016/S0960-894X(99)00257-7

Reference yield:

: 98272-33-4
methyl 3-cyclopropylacrylate

: 178247-85-3
C₄₁H₄₇Cl₆NO₁₆

Guidance literature:: Multi-step reaction with 9 steps

1: 48 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / Ambient temperature

2: 81 percent / NEt₃ / CH₂Cl₂ / 42 h / 0 °C

3: 100 percent / aq. K₂CO₃ / acetonitrile / 24 h / 50 °C

4: 81 percent / aq. NaN₃, HCO₂Me / methanol / 14 h / 50 °C

5: 96 percent / H₂ / Pd/C / ethyl acetate / 2.5 h / Ambient temperature

6: 96 percent / PPTS / toluene / 1.5 h / 80 °C

7: 100 percent / aq. LiOH / methanol / 1 h / Ambient temperature

8: 100 percent / DCC, DMAP / toluene / 1.4 h / 80 °C

9: 97 percent / HCO₂H / 2 h / Ambient temperature

With dmap; lithium hydroxide; formic acid; sodium azide; Methyl formate; AD-mix-β; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0960-894X(99)00257-7

Reference yield:

: 178248-34-5,238413-45-1
methyl (2R,3R)-3-cyclopropyl-2,3-epoxypropionate

: 178247-85-3
C₄₁H₄₇Cl₆NO₁₆

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / aq. NaN₃, HCO₂Me / methanol / 14 h / 50 °C

2: 96 percent / H₂ / Pd/C / ethyl acetate / 2.5 h / Ambient temperature

3: 96 percent / PPTS / toluene / 1.5 h / 80 °C

4: 100 percent / aq. LiOH / methanol / 1 h / Ambient temperature

5: 100 percent / DCC, DMAP / toluene / 1.4 h / 80 °C

6: 97 percent / HCO₂H / 2 h / Ambient temperature

With dmap; lithium hydroxide; formic acid; sodium azide; Methyl formate; hydrogen; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate; toluene;
DOI:10.1016/S0960-894X(99)00257-7