2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

Base Information

Chemical Name:2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide
CAS No.:326474-21-9
Molecular Formula:C₂₀H₃₄NO₃
Molecular Weight:336.495
Hs Code.:

Synonyms:2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

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Technology Process of 2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

There total 1 articles about 2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1219693-70-5
C₂₀H₃₃NO₃

: 326474-21-9
2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

Guidance literature:: With ammonia; oxygen; copper diacetate; In methanol; water; for 1h;
DOI:10.1039/b902636c

Reference yield: 80.0%

: 326474-21-9
2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1174281-56-1
N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

Guidance literature:: 2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide; 4-Vinylbenzyl chloride; With air; In isopropyl alcohol; toluene; for 1h;

With sodium tetrahydroborate; air; (-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III); In isopropyl alcohol; toluene;
DOI:10.1039/b902636c