N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

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Chemical Name:N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine
CAS No.:1174281-56-1
Molecular Formula:C₂₉H₄₂ClNO₃
Molecular Weight:488.11
Hs Code.:

Synonyms:N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

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Chemical Property of N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

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Technology Process of N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

There total 1 articles about N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 326474-21-9
2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1174281-56-1
N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

Guidance literature:: 2,2,5-trimethyl-4-[4'-(tetrahydropyran-2''-yloxymethyl)phenyl]-3-azahexane-3-nitroxide; 4-Vinylbenzyl chloride; With air; In isopropyl alcohol; toluene; for 1h;

With sodium tetrahydroborate; air; (-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III); In isopropyl alcohol; toluene;
DOI:10.1039/b902636c

Reference yield: 62.0%

: 1174281-56-1
N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

: 128143-88-4
2,2':6',2''-Terpyridin-4'(1'H)-one

: 1174281-57-2
O-(1-(4-((2,2':6',2''-terpyridin-4'-yloxy)methyl)phenyl)ethyl)-N-(tert-butyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)-oxy)methyl)phenyl)propyl)hydroxylamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 - 60 ℃; Inert atmosphere;
DOI:10.1039/b902636c

Reference yield:

: 1174281-56-1
N-(tert-butyl)-O-(1-(4-(chloromethyl)phenyl)ethyl)-N-(2-methyl-1-(4-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)propyl)hydroxylamine

: 1219696-65-7
(4-(1-((1-(4-((2,2':6',2''-terpyridin-4'-yloxy)methyl)phenyl)ethoxy)(tert-butyl)amino)-2-methylpropyl)phenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 60 °C

2: toluene-4-sulfonic acid / methanol; tetrahydrofuran / 18 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/pola.26586