[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

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Chemical Name:[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid
CAS No.:181697-10-9
Molecular Formula:C₂₅H₂₄N₂O₅S
Molecular Weight:464.542
Hs Code.:

Synonyms:[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

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Chemical Property of [4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

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Technology Process of [4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

There total 7 articles about [4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: C₂₅H₂₆N₂O₆S

: 181697-10-9
[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

Guidance literature:: With sulfuric acid; In tetrahydrofuran; for 2h; Heating / reflux;

Reference yield:

: 181697-07-4
2-[4-[N-[2,5-dimethylpyrrol]-sulfonyl]phenyl]-1-phenyl-ethan-1-one oxime

: 181697-10-9
[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

1.2: 2 h / -40 - 20 °C

2.1: sulfuric acid / tetrahydrofuran / 2 h / Heating / reflux

With n-butyllithium; sulfuric acid; In tetrahydrofuran;

Reference yield:

: 2,5-dimethyl-1-[[4-(2-oxo-2-phenylethyl)phenyl]sulfonyl]-1H-pyrrole

: 181697-10-9
[4-[4-[N-[2,5-dimethylpyrrol]sulfonyl]phenyl]-3-phenylisoxazol-5-yl]butan-1-oic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; sodium acetate / 14 h / Heating / reflux

2.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C

2.2: 2 h / -40 - 20 °C

3.1: sulfuric acid / tetrahydrofuran / 2 h / Heating / reflux

With n-butyllithium; sulfuric acid; hydroxylamine hydrochloride; sodium acetate; In tetrahydrofuran;