ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

Base Information

Chemical Name:ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate
CAS No.:150454-85-6
Molecular Formula:C₁₂H₁₀N₄O₆
Molecular Weight:306.235
Hs Code.:

Synonyms:ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

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Technology Process of ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

There total 3 articles about ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 114098-35-0
amino-(2-nitro-phenylhydrazono)-acetic acid ethyl ester

: 4755-77-5
Ethyl oxalyl chloride

: 150454-85-6
ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

: 150454-80-1
diethyl 1-(2-nitrophenyl)-1,2,4-triazole-3,5-dicarboxylate

Guidance literature:: With triethylamine; In benzene; for 8h; Heating;

Reference yield: 52.0%

: 150454-79-8
ethyl N¹-(2-nitrophenyl)-N³-ethoxalyloxamidrazonate

: 150454-85-6
ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

Reference yield:

: 114098-35-0
amino-(2-nitro-phenylhydrazono)-acetic acid ethyl ester

: 150454-85-6
ethyl 1,4,5,6-tetrahydro-1-(2-nitrophenyl)-5,6-dioxo-1,2,4-triazine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / diethyl ether; toluene / 0.25 h / Heating

2: 52 percent / triethylamine / dimethylformamide / 24 h / 80 °C

With triethylamine; In diethyl ether; N,N-dimethyl-formamide; toluene;