(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

Base Information

Chemical Name:(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane
CAS No.:104393-93-3
Molecular Formula:C₁₃H₂₅BO₃
Molecular Weight:240.151
Hs Code.:

Synonyms:(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

Suppliers and Price of (methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

Chemical Property:

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Technology Process of (methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

There total 1 articles about (methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 917-54-4
methyllithium

: 97235-25-1
(1'S,2'S)-(+)-2-(trans-2'-methylcyclohexyl)-1,3,2-dioxaborinane

: 104393-93-3
(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

Guidance literature:: In not given;
DOI:10.1021/ja00252a018

Reference yield:

: 4885-02-3
Dichloromethyl methyl ether

: 104393-93-3
(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

: 540-88-5
acetic acid tert-butyl ester

: 16047-06-6
<1S,2S>-(+)-trans-2-methylcyclohexyl methyl ketone

Guidance literature:: With dihydrogen peroxide; lithium tert-butoxide; Yield given; 1.) diethyl ether, r.t., 1 h, 2.) diethyl ether, pH 8 phosphate buffer, 12 h;
DOI:10.1021/ja00252a018

Reference yield:

: 104393-93-3
(methyl)(<1S,2S>-trans-2-methylcyclohexyl)(3-(trimethylsiloxy)propoxy)borane

: <1S,2S>-(+)-trans-2-methylcyclohexylamine hydrochloride

Guidance literature:: With water; hydroxylamine-O-sulfonic acid; Yield given. Multistep reaction; 1.) THF, 25 deg C, 12 h; 2.) diethyl ether;
DOI:10.1021/ja00281a050