N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

Base Information

Chemical Name:N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine
CAS No.:1427036-53-0
Molecular Formula:C₂₈H₄₀BNO₂
Molecular Weight:433.442
Hs Code.:

Synonyms:N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

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Chemical Property of N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

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Technology Process of N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

There total 2 articles about N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 695-12-5,25498-06-0
vinylcyclohexane

: 52742-32-2
N,N-dibenzyl-O-benzoylhydroxylamine

: 73183-34-3
bis(pinacol)diborane

: 1427036-53-0
N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

Guidance literature:: With chloro(4,5-bis(diphenylphosphano)-9,9-dimethylxanthene)copper(I); sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 4h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.5b02775

Reference yield:

: 695-12-5,25498-06-0
vinylcyclohexane

: 52742-32-2
N,N-dibenzyl-O-benzoylhydroxylamine

: 73183-34-3
bis(pinacol)diborane

: 1427036-53-0
N,N-dibenzyl-1-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethanamine

: 1427036-54-1
N,N-dibenzyl-2-cyclohexyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethan-1-amine

Guidance literature:: With o-phenylenebis(diphenylphosphine); copper(l) chloride; lithium tert-butoxide; In tetrahydrofuran; at 20 ℃; for 4h; Overall yield = 67 %; regioselective reaction;
DOI:10.1021/ja4007645