2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

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Chemical Name:2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione
CAS No.:507473-32-7
Molecular Formula:C₄₈H₄₅NO₇
Molecular Weight:747.888
Hs Code.:

Synonyms:2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

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Chemical Property of 2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

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Technology Process of 2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

There total 5 articles about 2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 189118-55-6
4-(2-{2-[2-(4-Trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenol

: 507473-32-7
2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

Guidance literature:: With potassium carbonate; In acetonitrile; for 48h; Heating;
DOI:10.1021/jo026370i

Reference yield:

: 31255-10-4
1,2-bis-(2-bromo-ethoxy)-ethane

: 507473-32-7
2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / K₂CO₃ / acetonitrile / 48 h / Heating

2: 78 percent / K₂CO₃ / acetonitrile / 24 h / Heating

3: 96 percent / H₂ / Pd/C / methanol; CH₂Cl₂ / 5 h / 827.44 Torr

4: 94 percent / K₂CO₃ / acetonitrile / 48 h / Heating

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo026370i

Reference yield:

: 978-86-9
4-tritylphenol

: 507473-32-7
2-{3-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-propyl}-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / K₂CO₃ / acetonitrile / 48 h / Heating

2: 78 percent / K₂CO₃ / acetonitrile / 24 h / Heating

3: 96 percent / H₂ / Pd/C / methanol; CH₂Cl₂ / 5 h / 827.44 Torr

4: 94 percent / K₂CO₃ / acetonitrile / 48 h / Heating

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo026370i