6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

Base Information

Chemical Name:6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one
CAS No.:758722-05-3
Molecular Formula:C₁₇H₁₈N₆OS
Molecular Weight:354.436
Hs Code.:

Synonyms:6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

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Chemical Property of 6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

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Technology Process of 6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

There total 8 articles about 6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162702-04-7
N-(4-cyano-3-methyl-1,2-thiazol-5-yl)-3-methylbutanamide

: 758722-05-3
6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium hydroxide; dihydrogen peroxide / water / 16 h / 60 °C

2: ammonium hydroxide / 5 h / 140 °C

3: potassium carbonate / N,N-dimethyl-formamide / 16 h / 25 °C

4: bromine; sodium acetate; acetic acid / 0.83 h / 100 °C

5: sodium azide / N,N-dimethyl-formamide / 1 h / 25 °C

With ammonium hydroxide; sodium azide; dihydrogen peroxide; bromine; sodium acetate; potassium carbonate; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm200629m

Reference yield:

: 162702-36-5
3-methyl-5-(3-methylbutanoylamino)-1,2-thiazole-4-carboxamide

: 758722-05-3
6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium hydroxide / 5 h / 140 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 25 °C

3: bromine; sodium acetate; acetic acid / 0.83 h / 100 °C

4: sodium azide / N,N-dimethyl-formamide / 1 h / 25 °C

With ammonium hydroxide; sodium azide; bromine; sodium acetate; potassium carbonate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm200629m

Reference yield:

: 5-benzyl-3-methyl-6-(2-methylpropyl)-[1,2]thiazolo[4,5-e]pyrimidin-4-one

: 758722-05-3
6-(1-azido-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; sodium acetate; acetic acid / 0.83 h / 100 °C

2: sodium azide / N,N-dimethyl-formamide / 1 h / 25 °C

With sodium azide; bromine; sodium acetate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm200629m