tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

Base Information

Chemical Name:tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate
CAS No.:758722-09-7
Molecular Formula:C₂₅H₃₅N₅O₃S
Molecular Weight:485.651
Hs Code.:

Synonyms:tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

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Chemical Property of tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

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Technology Process of tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

There total 14 articles about tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 758722-07-5
6-(1-amino-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

: 153815-24-8
1-(tert-butyloxycarbonylamino)-3,3-diethoxypropane

: 758722-09-7
tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

Guidance literature:: 6-(1-amino-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one; 1-(tert-butyloxycarbonylamino)-3,3-diethoxypropane; In toluene; at 20 ℃; Molecular sieve;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; toluene;

With acetic acid; In tetrahydrofuran; water; toluene; at 20 ℃; for 0.333333h;

Reference yield:

: C₂₅H₃₃N₅O₃S

: 758722-09-7
tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 758722-07-5
6-(1-amino-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one

: 58885-60-2
N-(tert-butoxycarbonyl)-3-aminopropanal

: 758722-09-7
tert-butyl N-[3-[[1-(5-benzyl-3-methyl-4-oxo-[1,2]thiazolo[5,4-d]pyrimidin-6-yl)-2-methylpropyl]amino]propyl]carbamate

Guidance literature:: 6-(1-amino-2-methylpropyl)-5-benzyl-3-methyl-[1,2]thiazolo[4,5-e]pyrimidin-4-one; N-(tert-butoxycarbonyl)-3-aminopropanal; In dichloromethane; at 20 ℃; for 3h; Molecular sieve;

With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; Product distribution / selectivity;