4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

Base Information

Chemical Name:4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)
CAS No.:1334149-62-0
Molecular Formula:C₂₅H₃₆Cl₂N₄O₈P₂
Molecular Weight:653.436
Hs Code.:

Synonyms:4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

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Chemical Property of 4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

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Technology Process of 4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

There total 3 articles about 4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 15285-42-4
benzyl nitrate

: 1346258-34-1
C₁₁H₂₄Cl₄N₂O₂P₂

: 1334149-62-0
4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm200521a

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 1346258-34-1
C₁₁H₂₄Cl₄N₂O₂P₂

: 1334149-62-0
4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

Guidance literature:: With N-ethyl-N,N-diisopropylamine; dmap; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: N-methyl-N-(4-chloro-n-butyl)amine hydrochloride

: 1334149-62-0
4-nitrobenzyl methylenebis(N-(4-chlorobutyl)-N-methylphosphonamidate)

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm200521a