N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

Base Information

Chemical Name:N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester
CAS No.:143182-17-6
Molecular Formula:C₃₂H₃₆N₂O₇
Molecular Weight:560.647
Hs Code.:

Synonyms:N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

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Chemical Property of N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

Chemical Property:

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Technology Process of N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

There total 1 articles about N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 69479-87-4
Malonic acid monobenzyl ester acid chloride

: 150107-61-2
N-<1-(2-Phenylaminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

: 143182-17-6
N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

Guidance literature:: In chloroform; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90208-X

Reference yield:

: 143182-17-6
N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

: N-[2-(tert-Butoxycarbonylmethyl-amino)-ethyl]-N-phenyl-malonamic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h; under 2585.7 Torr; Ambient temperature;
DOI:10.1016/S0040-4020(01)90208-X

Reference yield:

: 143182-17-6
N-<1-(2-Phenyl-(N-benzylmalonyl)-aminoethyl)>-N-benzyloxycarbonyl-glycine t-butyl ester

: 143148-29-2
1-Phenyl-2,4-dioxo-5-methyl-hexahydro-1,5-diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5 percent Pd/C / methanol / 4 h / 2585.7 Torr / Ambient temperature

2: diphenylphosphoryl azide / dimethylformamide / 72 h / Ambient temperature

With diphenylphosphoranyl azide; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)90208-X