{NEt₄}{Co(CO)4}

Base Information

Chemical Name:{NEt₄}{Co(CO)4}
CAS No.:29477-07-4
Molecular Formula:C₄CoO₄*C₈H₂₀N
Molecular Weight:301.288
Hs Code.:

Synonyms:{NEt₄}{Co(CO)4}

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Chemical Property of {NEt₄}{Co(CO)4}

Chemical Property:

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Technology Process of {NEt₄}{Co(CO)4}

There total 6 articles about {NEt₄}{Co(CO)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 68-05-3
tetraethylammonium iodide

: 113109-28-7
{Pd₂CoI(CO)3(dppm)2}

: 29477-07-4
{NEt₄}{Co(CO)4}

Guidance literature:: In dichloromethane; A soln. of {NEt4}I in CH2Cl2 was added to a soln. of {Pd2Co2(CO)7(dppm)2} in CH2Cl2.; Addn. of n-C6H14 to the soln. and cooling (-20°C) gave a ppt. of {NEt4}I (removed by filtration). More n-C6H14 was then added to the soln. and afforded a powder contg. {NEt4}{Co(CO)4} and {Pd2Co(CO)3(dppm)2I} (fractional crystn.).;

Reference yield: 40.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: {W(CC6H4Me-2)(CO)2(η5-C2B9H9Me2)}NEt4

: 14040-11-0
tungsten hexacarbonyl

: 29477-07-4
{NEt₄}{Co(CO)4}

: 15041-50-6
Co₄(CO)12

: NEt4{Co2W(μ3-CC6H4Me-2)(CO)6(η5-C2B9H9)}

Guidance literature:: In dichloromethane; stirring under slow stream of N2 for ca 24 h; evapn. redissolving in CH2Cl2, chromy. (alumina, CH2Cl2), concn. of dark brown eluate, addn. of light petroleum, oil redissolved in CH2Cl2, trichloroethylene added, cooled to -20°C, elem. anal.;

Reference yield: 39.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: NEt4{W(CPh)(CO)2(η5-C2B9H9Me2)}

: 14040-11-0
tungsten hexacarbonyl

: 29477-07-4
{NEt₄}{Co(CO)4}

: 15041-50-6
Co₄(CO)12

: NEt4{Co2W(μ3-CPh)(CO)6(η5-C2B9H9Me2)}

Guidance literature:: In dichloromethane; stirring under slow stream of N2 for 24 h; evapn., redissolving in CH2Cl2, chromy. (alumina, CH2Cl2), addn. of light petroleum to dark brown eluate, oil redissolved in CH2Cl2, trichloroethylene added, crystn. of Co2W-complex at -20°C, elem. anal.;