C₃₅H₅₅NO₄Si₂

Base Information

Chemical Name:C₃₅H₅₅NO₄Si₂
CAS No.:1265214-95-6
Molecular Formula:C₃₅H₅₅NO₄Si₂
Molecular Weight:609.997
Hs Code.:

C<sub>35</sub>H<sub>55</sub>NO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₅H₅₅NO₄Si₂

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Chemical Property of C₃₅H₅₅NO₄Si₂

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Technology Process of C₃₅H₅₅NO₄Si₂

There total 10 articles about C₃₅H₅₅NO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 994-30-9
triethylsilyl chloride

: 1265215-32-4
C₂₉H₄₁NO₄Si

: 1265214-95-6
C₃₅H₅₅NO₄Si₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ol103024z

Reference yield:

: 1033282-40-4
diethyl 4-ethylideneheptanedioate

: 1265214-95-6
C₃₅H₅₅NO₄Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.1: 1H-imidazole / dichloromethane / 2 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C

3.2: 0.5 h / -78 °C

4.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

5.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

6.1: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

9.1: dmap; triethylamine / dichloromethane / 4 h / 20 °C

With 1H-imidazole; dmap; lithium aluminium tetrahydride; oxalyl dichloride; potassium trimethylsilonate; palladium diacetate; potassium hexamethylsilazane; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Horner-Wadsworth-Emmons olefination / 5.1: Mizoroki-Heck cyclization;
DOI:10.1021/ol103024z

Reference yield:

: 1265214-87-6
C₂₅H₃₄O₂Si

: 1265214-95-6
C₃₅H₅₅NO₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

3: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

5: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

6: dmap; triethylamine / dichloromethane / 4 h / 20 °C

With dmap; potassium trimethylsilonate; palladium diacetate; potassium hexamethylsilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 1: Horner-Wadsworth-Emmons olefination / 2: Mizoroki-Heck cyclization;
DOI:10.1021/ol103024z