C₉H₁₁ClZn

Base Information

• Chemical Name: C₉H₁₁ClZn
• CAS No.: 1165947-04-5
• Molecular Formula: C₉H₁₁ClZn
• Molecular Weight: 220.029
• Mol file: 1165947-04-5.mol

Synonyms:C₉H₁₁ClZn

Chemical Property of C₉H₁₁ClZn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₉H₁₁ClZn

There total 1 articles about C₉H₁₁ClZn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-2-isopropylbenzene (7073-94-1) + zinc(II) chloride (7646-85-7,24359-56-6) → C9H11ClZn (1165947-04-5)

Guidance literature:

1-bromo-2-isopropylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; for 1h; Inert atmosphere; Cooling with acetone-dry ice;

zinc(II) chloride; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.orglett.5b01540

Reference yield:

C9H11ClZn (1165947-04-5) → o-cumenesulfonyl chloride (61738-47-4)

Guidance literature:

With 2,4,6-trichlorophenyl chlorosulfate; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/acs.orglett.5b01540

Reference yield:

C9H11ClZn (1165947-04-5) → N-benzyl-2-isopropylbenzenesulfonamide

Guidance literature:

Multi-step reaction with 2 steps

1: 2,4,6-trichlorophenyl chlorosulfate / tetrahydrofuran; hexane; 2-methyltetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran; hexane; 2-methyltetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

With 2,4,6-trichlorophenyl chlorosulfate; In tetrahydrofuran; 2-methyltetrahydrofuran; hexane;

DOI:10.1021/acs.orglett.5b01540

upstream raw materials:

1-bromo-2-isopropylbenzene

zinc(II) chloride

Downstream raw materials:

o-cumenesulfonyl chloride

Refernces