O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate

Base Information

Chemical Name:O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate
CAS No.:1254063-71-2
Molecular Formula:C₁₈H₁₉NO₂S₂
Molecular Weight:345.486
Hs Code.:

Synonyms:O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate

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Technology Process of O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate

There total 1 articles about O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67237-53-0
3-ethynylthiophene

: 1254063-64-3
O-3-bromo-2-(methylthio)phenyl N,N-diethylcarbamate

: 1254063-71-2
O-2-(methylthio)-3-[2-(thiophen-3-yl)ethynyl]phenyl N,N-diethylcarbamate

Guidance literature:: O-3-bromo-2-(methylthio)phenyl N,N-diethylcarbamate; With dichloro bis(acetonitrile) palladium(II); caesium carbonate; XPhos; In acetonitrile; at 20 ℃; for 0.416667h; Inert atmosphere;

3-ethynylthiophene; In acetonitrile; at 85 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo101436f