allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone

Base Information

• Chemical Name: allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone
• CAS No.: 121720-83-0
• Molecular Formula: C₁₅H₂₃ClN₂O₄
• Molecular Weight: 330.812
• Mol file: 121720-83-0.mol

Synonyms:allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone

Chemical Property of allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone

There total 3 articles about allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

t-butoxycarbonylhydrazine (870-46-2) + allyl 1-chloro-2-oxocyclohexanecarboxylate (121720-80-7) → allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone (121720-83-0)

Guidance literature:

With acetic acid; In diethyl ether; for 24h;

Reference yield:

pimelic acid diallyl ester (91906-66-0) → allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone (121720-83-0)

Guidance literature:

Multi-step reaction with 3 steps

2: 90 percent / sulphuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 15 h, 2.) room temperature, 4 h

3: 60 percent / acetic acid / diethyl ether / 24 h

With sulfuryl dichloride; acetic acid; In diethyl ether; dichloromethane;

Reference yield:

allyl 2-oxocyclohexane-1-carboxylate (5453-93-0) → allyl 1-chloro-2-oxocyclohexanecarboxylate t-butoxycarbonylhydrazone (121720-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / sulphuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 15 h, 2.) room temperature, 4 h

2: 60 percent / acetic acid / diethyl ether / 24 h

With sulfuryl dichloride; acetic acid; In diethyl ether; dichloromethane;

upstream raw materials:

t-butoxycarbonylhydrazine

allyl 1-chloro-2-oxocyclohexanecarboxylate

pimelic acid diallyl ester

allyl 2-oxocyclohexane-1-carboxylate

Downstream raw materials:

allyl 2-(t-butoxycarbonylazo)cyclohex-1-ene-1-carboxylate