rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

Base Information

Chemical Name:rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane
CAS No.:405072-09-5
Molecular Formula:C₁₆H₂₂GeO₂
Molecular Weight:318.939
Hs Code.:

Synonyms:rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

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Chemical Property of rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

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Technology Process of rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

There total 1 articles about rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 405072-08-4
rac-(chloromethyl)cyclopentyl(phenyl)vinylgermane

: 127-09-3
sodium acetate

: 405072-09-5
rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

Guidance literature:: In N,N-dimethyl-formamide; (N2); mixt. of Ge compd. and AcONa in DMF was stirred under reflux for 5h; cooled to room temp.; filtered; solvent removed (vac.); residue distd. (vac.); elem. anal.;
DOI:10.1016/S0022-328X(01)01179-2

Reference yield: 92.0%

: 405072-09-5
rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

: 7732-18-5
water

: 405072-10-8
rac-cyclopentyl(hydroxymethyl)phenyl(vinyl)germane

Guidance literature:: With LiAlH₄; HCl; In diethyl ether; (N2); soln. of Ge compd. in Et2O was added dropwise to stirred suspn. ofLiAlH4 in Et2O at -30°C within 2 h; mixt. was stirred at -30.deg ree.C for 1 h and added to ice-cooled HCl; org. phase septd.; aq. layer extd. (Et2O); org. ext. dried (Na2SO4); solvent removed (vac.); residue distd. (vac.); elem. anal.;
DOI:10.1016/S0022-328X(01)01179-2

Reference yield:

: 405072-09-5
rac-(acetoxymethyl)cyclopentyl(phenyl)vinylgermane

: 405072-11-9
rac-cyclopentyl(phenyl)[(trimethylsilyloxy)methyl]vinylgermane

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; HCl / diethyl ether

2: Et₃N / pentane

With LiAlH₄; HCl; Et₃N; In diethyl ether; pentane;
DOI:10.1016/S0022-328X(01)01179-2