((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

Base Information

Chemical Name:((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside
CAS No.:1253373-80-6
Molecular Formula:C₂₀H₂₈N₆O₉S
Molecular Weight:528.543
Hs Code.:

Synonyms:((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

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Chemical Property of ((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

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Technology Process of ((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

There total 1 articles about ((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 443864-69-5
methyl 2,4,6-tri-O-acetyl-3-azido-3-deoxy-1-thio-β-D-galactospyranoside

: 1253373-79-3
(1R,2S,6S)-2-azido-6-hydroxycyclohexyl acetate

: 1253373-80-6
((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

Guidance literature:: (1R,2S,6S)-2-azido-6-hydroxycyclohexyl acetate; With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -10 ℃; for 1h;

methyl 2,4,6-tri-O-acetyl-3-azido-3-deoxy-1-thio-β-D-galactospyranoside; With triethylamine; In dichloromethane; for 16h;

Reference yield: 93.0%

: 1253373-80-6
((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

: 766-49-4
(2-fluorophenyl)acetylene

: 1253373-81-7
((1R,2R,3S)-2-acetoxy-3-(4-(2-fluorophenyl)-1H-1,2,3-triazol-1-yl)cyclohexyl) 2,4,6-tri-O-acetyl-3-deoxy-3-(4-(2-fluorophenyl)-1H-1,2,3-triazol-1-yl)-1-thio-β-D-galactopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; copper(l) iodide; In toluene; at 45 ℃; for 22h;

Reference yield:

: 1253373-80-6
((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside

: 1253373-91-9
((1R,2R,3S)-2-hydroxy-3-azidocyclohexyl)-3-deoxy-3-azido-thio-β-D-galactopyranoside

Guidance literature:: ((1R,2R,3S)-2-acetoxy-3-azidocyclohexyl) 2,4,6-tri-O-acetyl-3-azido-3-deoxy 1-thio-β-D-galactopyranoside; With sodium methylate; In methanol; dichloromethane;