(2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester

Base Information

• Chemical Name: (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester
• CAS No.: 1021491-65-5
• Molecular Formula: C₁₆H₂₄O₄
• Molecular Weight: 280.364

Synonyms:(2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester

Chemical Property of (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester

Chemical Property:

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Technology Process of (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester

There total 1 articles about (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1,1-dimethylethyl)[[(Z)-1-(1-ethyl-1-methylpropoxy)-2-methoxyethenyl]oxy](dimethyl)silane + benzaldehyde (100-52-7) → (2R,3R)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester + (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester (1021491-65-5)

Guidance literature:

With tetrachlorosilane; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 0.5h; Title compound not separated from byproducts.;

DOI:10.1021/jo8006539

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + (2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester (1021491-65-5) → (2S,3S)-2,3-dihydroxy-3-phenylpropanoic acid methyl ester

Guidance literature:

(2S,3S)-3-hydroxy-2-methoxy-3-phenylpropanoic acid 1-ethyl-1-methylpropyl ester; With aluminium trichloride; n-butanethiol; at 20 ℃; for 24h;

diazomethane; In diethyl ether; at 0 ℃; for 0.166667h; Further stages.;

DOI:10.1021/jo8006539

upstream raw materials:

benzaldehyde

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