1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

Base Information

Chemical Name:1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate
CAS No.:1093865-10-1
Molecular Formula:C₁₅H₂₈N₄O₂
Molecular Weight:296.413
Hs Code.:

Synonyms:1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

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Chemical Property of 1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

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Technology Process of 1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

There total 5 articles about 1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 884511-11-9
(S)-tert-butyl (1-azido-3-cyclohexylpropan-2-yl)carbamate

: 74-88-4
methyl iodide

: 1093865-10-1
1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

Guidance literature:: (S)-tert-butyl (1-azido-3-cyclohexylpropan-2-yl)carbamate; With sodium hydride; In N,N-dimethyl-formamide;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

Reference yield:

: 103322-56-1
tert-butyl [(1S)-2-cyclohexyl-1-(hydroxymethyl)ethyl]carbamate

: 1093865-10-1
1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.83 h / 0 - 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide

3.2: 1.5 h / 20 °C

With sodium azide; sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1093865-10-1
1,1-dimethylethyl [(1S)-2-azido-1-(cyclohexylmethyl)ethyl]methylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / 1,4-dioxane; water / 0 - 20 °C

2.1: triethylamine / dichloromethane / 0.83 h / 0 - 20 °C

3.1: sodium azide / N,N-dimethyl-formamide / 80 °C

4.1: sodium hydride / N,N-dimethyl-formamide

4.2: 1.5 h / 20 °C

With sodium azide; sodium hydride; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;