C₁₅H₂₄O₄S

Base Information

• Chemical Name: C₁₅H₂₄O₄S
• CAS No.: 912293-21-1
• Molecular Formula: C₁₅H₂₄O₄S
• Molecular Weight: 300.419
• Mol file: 912293-21-1.mol

Synonyms:C₁₅H₂₄O₄S

Chemical Property of C₁₅H₂₄O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₄O₄S

There total 9 articles about C₁₅H₂₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H30O2Si (912293-19-7) → C15H24O4S (912293-21-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 97 percent / pyridine / 16 h / 0 - 20 °C

2: 94 percent / HF*Py / tetrahydrofuran / 14 h / 20 °C

3: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2.5 h / -78 - 20 °C

4: tetrahydrofuran / 3.5 h / -78 - -50 °C

With oxalyl dichloride; pyridine hydrogenfluoride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; 3: Swern oxidation;

DOI:10.1055/s-2006-942459

Reference yield:

C20H36O4SSi (912293-10-8) → C15H24O4S (912293-21-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / HF*Py / tetrahydrofuran / 14 h / 20 °C

2: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2.5 h / -78 - 20 °C

3: tetrahydrofuran / 3.5 h / -78 - -50 °C

With oxalyl dichloride; pyridine hydrogenfluoride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 2: Swern oxidation;

DOI:10.1055/s-2006-942459

Reference yield:

C14H22O4S (912293-20-0) → C15H24O4S (912293-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2.5 h / -78 - 20 °C

2: tetrahydrofuran / 3.5 h / -78 - -50 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 1: Swern oxidation;

DOI:10.1055/s-2006-942459

upstream raw materials:

C₁₄H₂₀O₄S

methylmagnesium chloride

C₁₄H₃₀O₃Si

C₁₃H₃₀O₂Si

Downstream raw materials:

C₁₅H₂₂O₄S