C₁₈H₂₈O

Base Information

Chemical Name:C₁₈H₂₈O
CAS No.:954106-18-4
Molecular Formula:C₁₈H₂₈O
Molecular Weight:260.42
Hs Code.:

Synonyms:C₁₈H₂₈O

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Chemical Property of C₁₈H₂₈O

Chemical Property:

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Technology Process of C₁₈H₂₈O

There total 4 articles about C₁₈H₂₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 179913-85-0
(2R,3S)-2,3,7-trimethyl-6-octen-1-ol

: 100-39-0
benzyl bromide

: 954106-18-4
C₁₈H₂₈O

Guidance literature:: (2R,3S)-2,3,7-trimethyl-6-octen-1-ol; With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 22 - 24 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja201254c

Reference yield:

: 954106-37-7
(4R,5S)-3-(3,7-dimethyloct-6-enoyl)-4-methyl-5-phenyl-2-oxazolidinone

: 954106-18-4
C₁₈H₂₈O

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilamide / tetrahydrofuran; toluene / 1 h / -78 °C

1.2: 83 percent / tetrahydrofuran; toluene / 3.5 h / -78 °C

2.1: 81 percent / NaBH₄ / tetrahydrofuran; H₂O / 5 h / 20 °C

3.1: NaH; imidazole / tetrahydrofuran / 0.5 h / 0 °C

3.2: 83 percent / tetrabutylammonium iodide / tetrahydrofuran / 3 h / 20 - 45 °C

With 1H-imidazole; sodium tetrahydroborate; sodium hexamethyldisilazane; sodium hydride; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-16-2
C₂₁H₂₉NO₃

: 954106-18-4
C₁₈H₂₈O

Guidance literature:: Multi-step reaction with 2 steps

1.1: 81 percent / NaBH₄ / tetrahydrofuran; H₂O / 5 h / 20 °C

2.1: NaH; imidazole / tetrahydrofuran / 0.5 h / 0 °C

2.2: 83 percent / tetrabutylammonium iodide / tetrahydrofuran / 3 h / 20 - 45 °C

With 1H-imidazole; sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2007.07.182