diphenylphosphinic acid triethylsilyl ester

Base Information

• Chemical Name: diphenylphosphinic acid triethylsilyl ester
• CAS No.: 124340-38-1
• Molecular Formula: C₁₈H₂₅O₂PSi
• Molecular Weight: 332.455
• Mol file: 124340-38-1.mol

Synonyms:diphenylphosphinic acid triethylsilyl ester

Chemical Property of diphenylphosphinic acid triethylsilyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of diphenylphosphinic acid triethylsilyl ester

There total 6 articles about diphenylphosphinic acid triethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

triethylsilanethiol (17145-35-6) + triphenylsilyldiphenylphosphinate (125722-48-7) → diphenyl-phosphinic acid (1707-03-5) + diphenylphosphinic acid triethylsilyl ester (124340-38-1)

Guidance literature:

In benzene; at 40 ℃; for 24h;

DOI:10.1016/S0040-4020(01)89077-3

Reference yield:

(Diphenylphosphinyloxy)trimethylsilan (18789-78-1) → diphenylphosphinic acid triethylsilyl ester (124340-38-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent

2: 40 percent / benzene / 24 h / 40 °C

In benzene;

DOI:10.1016/S0040-4020(01)89077-3

Reference yield:

Diphenylphosphinic chloride (1499-21-4) → diphenylphosphinic acid triethylsilyl ester (124340-38-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / cyclohexane / Heating

2: Et₃N / CDCl₃

With water; triethylamine; In chloroform-d1; cyclohexane;

DOI:10.1021/jo00289a042

upstream raw materials:

triethylsilanethiol

triphenylsilyldiphenylphosphinate

triethylsilyl chloride

diphenyl-phosphinic acid