TG-mPhos

Base Information

Chemical Name:TG-mPhos
CAS No.:1253913-12-0
Molecular Formula:C₂₂H₁₉O₈P
Molecular Weight:442.362
Hs Code.:

Synonyms:TG-mPhos

Suppliers and Price of TG-mPhos

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TG-mPhos

Chemical Property:

Purity/Quality:

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Technology Process of TG-mPhos

There total 3 articles about TG-mPhos which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1253913-11-9
C₃₆H₃₁O₈P

: 1253913-12-0
TG-mPhos

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja201028t

Reference yield:

: 1253913-13-1
2-Me-4-OMe TokyoGreen-methyleneoxy phosphorylcholine

: 1253913-12-0
TG-mPhos

Guidance literature:: Multi-step reaction with 3 steps

1: recombinant pyrophosphatase/phosphodiesterase-6 / dimethyl sulfoxide / 20 °C / pH 9 / Alkaline aq. solution; Enzymatic reaction

2: caesium carbonate / N,N-dimethyl-formamide / 13 h / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 1 h / 20 °C

With palladium 10% on activated carbon; recombinant pyrophosphatase/phosphodiesterase-6; hydrogen; caesium carbonate; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja201028t

Reference yield:

: 643755-84-4
6-hydroxy-9-(4-methoxy-2-methylphenyl)-3H-xanthene-3-one

: 1253913-12-0
TG-mPhos

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 13 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 1 h / 20 °C

With palladium 10% on activated carbon; hydrogen; caesium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja201028t