3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)-

Base Information

Chemical Name:3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)-
CAS No.:643755-84-4
Molecular Formula:C21H16O4
Molecular Weight:332.356
Hs Code.:

Synonyms:

Suppliers and Price of 3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of 3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)-

Chemical Property:

Purity/Quality:: 99.3% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)-

There total 11 articles about 3H-Xanthen-3-one, 6-hydroxy-9-(4-methoxy-2-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 148706-30-3
2-methyl-4-methoxyphenylmagnesium bromide

: 121714-18-9
3,6-bis(tert-butyldimethylsilyloxy)-9H-xanthen-9-one

: 643755-84-4
6-hydroxy-9-(4-methoxy-2-methylphenyl)-3H-xanthene-3-one

Guidance literature:: 2-methyl-4-methoxyphenylmagnesium bromide; 3,6-bis(tert-butyldimethylsilyloxy)-9H-xanthen-9-one; In tetrahydrofuran; at 0 ℃; for 0.166667h;

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1021/ja043919h

Reference yield: 68.0%

: 27060-75-9
4-bromo-3-methylanisole

: 121714-18-9
3,6-bis(tert-butyldimethylsilyloxy)-9H-xanthen-9-one

: 643755-84-4
6-hydroxy-9-(4-methoxy-2-methylphenyl)-3H-xanthene-3-one

Guidance literature:: 4-bromo-3-methylanisole; With magnesium; In tetrahydrofuran; at 60 ℃; for 5h; Inert atmosphere;

3,6-bis(tert-butyldimethylsilyloxy)-9H-xanthen-9-one; In tetrahydrofuran; for 0.5h; Inert atmosphere; Cooling with ice;

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 15h; Cooling with ice;

Reference yield:

: TG-Phos

: 643755-84-4
6-hydroxy-9-(4-methoxy-2-methylphenyl)-3H-xanthene-3-one

Guidance literature:: With hydrogenchloride; 2-amino-2-hydroxymethyl-1,3-propanediol; Alkaline phosphatase EC 3.1.3.1; magnesium chloride; at 37 ℃; pH=7.4;
DOI:10.1002/anie.200501542