methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

Base Information

Chemical Name:methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside
CAS No.:769126-80-9
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

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Chemical Property of methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

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Technology Process of methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

There total 2 articles about methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₃BO₅

: 769126-80-9
methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.bmc.2007.12.039

Reference yield:

: 3150-15-0,3150-16-1,3257-59-8,14187-71-4,15384-57-3,19465-13-5,32976-15-1,52885-37-7,53270-02-3,53270-03-4,65391-11-9,65391-12-0,66537-92-6,67226-04-4,71184-14-0,86420-78-2,86420-79-3,91177-51-4,91177-52-5,117708-93-7,120408-72-2,2880-96-8
methyl 2,3-anhydro-4,6-O-benzilidene-α-D-mannopyranoside

: 769126-80-9
methyl 4,6-O-benzylidene-3-deoxy-3-C-(3-hydroxypropyl)-α-D-altopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / tetrahydrofuran / 1 h / 80 °C

2.1: BH₃*THF / tetrahydrofuran / 23 h / 20 °C

2.2: 91 percent / aq. H₂O₂; aq. NaOH / 3 h / 20 °C

With borane-THF; In tetrahydrofuran;
DOI:10.1016/j.tet.2004.05.113